摘要 利用CaCl2、NH4H22PO4、NH3·H2O和Al(NO3)3溶液为原料，在高温、高压条件下快速水热制取羟基磷石灰，并用红外(IR)、X射线衍射(XRD)分析和表征羟基磷灰石晶体的结构及其结晶度。结果表明，用该法制备的羟基磷石灰晶体有较好的结晶度，且该法制备过程简单、制备时间短。
关键词 水热法 羟基磷石灰 铝离子
Preparation of Al-Doped Hydroxyapatite by Rapid Hydrothermal Method
HONG Liu， LIN Changchun， YU Wenli， ZHAO Yaping
( School of Chemistry and Chemical Engineering，Shanghai Jiaotong University，Shanghai 200240)
Abstract Using NH4H22PO4、NH3·H2O和Al(NO3)3 solution as the raw materials, hydroxyapatite is prepared at high temperature and high pressure by the rapid hydrothermal method. IR and XRD are used to analyze and characterize the structure and crystallinity of the obtained samples. The result shows that hydroxyapatite which is prepared by this method has a good crystallinity, and this method is very easy in the process, which takes a short time.
Keywords hydrothermal method, hydroxyapatite, aluminum ion